Polarimetric determination of boric acid with mannitol
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چکیده
منابع مشابه
Chelation of boric acid with some nucleosides.
Tab. 1. NMR-Spektren substituierter Acetanilide a . a In CDC13 , 60 MHz. b Die Zuordnung erfolgte unter der plausiblen Annahme, daß in der eis-Verbindung der Methylteil der CH3CO-Gruppe oberhalb der aromatischen Ringebene zu liegen kommt, ihr NMR-Signal im Vergleich zur fransVerbindung also nach höherem Feld verschoben sein sollte. c Im Falle des cts-2.6-Diisopropyl-acetanilides zeigen die iso-...
متن کاملEffect of pretreating samples with boric acid before liquid-chromatographic determination of urinary catecholamines.
Isolation of catecholamines on prepacked gravity-fed ion-exchange columns in conjunction with liquid-chromatographic separation is occasionally subject to disturbances of unknown origin, especially after injection of H3BO3 eluates from the ion-exchange columns onto the chromatography column. Peak spreading, sometimes even peak splitting, has been observed in many laboratories--effects easily co...
متن کاملReproductive toxicology. Boric acid.
Boric acid (BA), widely used for both medicinal and nonmedicinal purposes, was known to adversely affect reproduction and fertility in rodents. NIOSH, in evaluating the literature prior to writing a Criteria Document, asked NIEHS to perform an RACB study on BA to generate both structural and functional data to be used for setting exposure criteria (Fail et al., Fundam Appl Toxicol 17:225-239 [1...
متن کاملBoric Acid and Borates
Boric acid and its chemical relatives are pesticides that are derived from the element boron. Boron rarely occurs alone and is typically found in combination with other elements; common combinations are boric acid or borates.1 Unlike many pesticides which are synthetic compounds,2 boric acid and related pesticides are naturally occurring compounds.1 Boron compounds are widely found in rivers, s...
متن کاملSimultaneous determination of catecholamines and serotonin by liquid chromatography, after treatment with boric acid gel.
We describe a liquid-chromatographic method for simultaneously determining norepinephrine, epinephrine, dopamine, and serotonin in 0.5 mL of human plasma. These analytes are purified on boric acid gel from Aldrich, separated on a reversed-phase C18 column, and detected electrochemically at +600 mV. Absolute recoveries of internal standards were 84% for 3,4-dihydroxybenzylamine and 57% for N-met...
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ژورنال
عنوان ژورنال: BUNSEKI KAGAKU
سال: 1960
ISSN: 0525-1931
DOI: 10.2116/bunsekikagaku.9.685